The synthesis of solid acid catalyst ZrO 2/ Fe 3O 4 applied in the synthesis of iso amyl acetate and the analysis of it by IR, TEM, XRD, DTA techniques were reported here. 合成了固体酸催化剂ZrO2/Fe3O4,对催化剂进行了IR,TEM,XRD,DTA分析,并用于催化合成乙酸异戊酯。
The synthesis of I amyl acetate from I amylic alcohol and acetic acid using silica gel carrier acid as catalyst is reported. 以乙酸和异戊醇为原料,采用硅胶载体酸为催化剂合成乙酸异戊酯。
Some technological conditions for the separation of spiramycin, using amyl acetate impregnated resin, were studied. 本文首次研究了醋酸戊酯浸渍树脂吸附分离螺旋霉素的工艺条件。
It is reported that fusel oil can be used for synthesising mixing esters mainly inclusding amyl acetate when it is heated and back-flowed with Catalyst oil of vitriol or canon exchange resin. 本文报告了以酒厂废料杂醇油为原料,在催化剂浓硫酸或阳离子交换树酯存在下,经加热回流与冰醋酸反应生成以乙酸异戊酯为主的混合酯。
The complex compound of Cr(ⅵ) and dimethylindodicarbocyanine ( DIDC) dye was extracted by amyl acetate in chloride ions containing acid solutions. Therefore a new method for Cr(ⅵ) determination was developed. 在含氯离子的酸性溶液中,用醋酸戊酯萃取二甲基吲哚二羰花青(DIDC)染料与Cr(Ⅵ)配合物,从而建立一种新的测定Cr(Ⅵ)的方法。
Tin tetrachloride can be used as catalyst for esterification reaction instead of sulfuric acid and it shows fine catalytic effect for the synthesis of iso amyl acetate, n amyl acetate and n butyl acetate. The yield can all get to 90% at reaction for 1 h. 四氯化锡取代浓硫酸作为酯化催化剂,在乙酸异戊酯、乙酸正戊酯、乙酸正丁酯的合成中显示出很好的催化效果,反应1h产率都可达90%以上。
The synthesis conditions of amyl acetate are studied in the presence of solid superacid AlCl_3.CuSO_4 as catalyst under microwave radiation. 在微波辐射下,以AlCl3.CuSO4固体超强酸为催化剂合成乙酸正戊酯。
H-β zeolite has been used for catalyzing the esterification reactions of acetic acid with n-butanol, and with n-pentanol, respectively. to synthesize butyl acetate and amyl acetate. 用H-β沸石作催化剂,对乙酸与正丁醇以及乙酸与正戊醇的酯化反应进行了研究。
Synthesis of Amyl Acetate Using SO_4~ ( 2-)/ TiO_2 as a Catalyst SO4~(2-)/TiO2催化合成乙酸戊酯
Firstly amyl acetate was selected as substrate in order to study optimized conditions, including catalysts, reaction time, reaction temperature, amount of sodium azide and amount of the metal catalyst. 首先我们选择醋酸正戊酯为底物,探讨该反应的催化剂、反应时间、反应温度、叠氮化钠用量、金属催化剂用量等合适的反应条件。